NMR of Quadrupolar Nuclei in Solid Materials.pdf

NMR of Quadrupolar Nuclei in Solid Materials PDF

Roderick E. Wasylishen

Over the past 20 years technical developments in superconducting magnet technology and instrumentation have increased the potential of NMR spectroscopy so that it is now possible to study a wide range of solid materials. In addition, one can probe the nuclear environments of many other additional atoms that possess the property of spin. In particular, it is possible to carry out NMR experiments on isotopes that have nuclear spin greater than 1/2 (i.e. quadrupolar nuclei). Since more than two-thirds of all NMR active isotopes are quadrupolar nuclei, applications of NMR spectroscopy with quadrupolar nuclei are increasing rapidly. The purpose of this handbook is to provide under a single cover the fundamental principles, techniques and applications of quadrupolar NMR as it pertains to solid materials. Each chapter has been prepared by an expert who has made significant contributions to our understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three sections : The first provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar nuclei in solids. The second presents cutting-edge techniques and methodology for employing these techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of dynamics, characterizations of biological samples, organic and inorganic materials, porous materials, glasses, catalysts, semiconductors and high-temperature superconductors.

Moreover, solid-state NMR may also unveil information across the “difficult” 0.3–1 nm length-scale, unlike other ... using solid-state two-dimensional NMR spectroscopy. J. S. Shorea) and S. H. Wang. Materials Science Division, Lawrence Berkeley Laboratory and Department of Chemistry, ... the NMR spectra of quadrupolar nuclei are still needed.

3.64 MB Taille du fichier
9780470973981 ISBN
Libre PRIX
NMR of Quadrupolar Nuclei in Solid Materials.pdf

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Sofya Voigtuh

NMR of Quadrupolar Nuclei in Solid Materials …

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Mattio Müllers

5 Sep 2002 ... High-Resolution NMR Spectroscopy of Quadrupolar Nuclei in Solids: ... for the study of quadrupolar nuclei in clays and other layered materials. Download Citation | Quadrupolar Nuclei in Solids | In this article, the reader is introduced to the fundamental ... Materials' Methods: NMR in Battery Research.

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Noels Schulzen

First and foremost, the practical motivation for the use of Czjzek model in the context of MAS NMR of quadrupolar nuclei is to provide a quadrupolar lineshape for disordered materials so as to be able to decompose quantitatively and accurately their spectra. After validating this approach on known samples, we now will show on a complex multi-phase sample how, from a simple one-pulse experiment NMR of Quadrupolar Nuclei in Solid Materials | NMR ...

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Jason Leghmann

Get this from a library! NMR of Quadrupolar Nuclei in Solid Materials. [Roderick E Wasylishen; Sharon E Ashbrook; Stephen Wimperis;] -- Many important materials do not contain spin-1/2 nuclei traditionally investigated by NMR spectroscopy and secondly, dissolving solid materials in a solvent may be impossible or may destroy the NMR of Quadrupolar Nuclei in Solid Materials …

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Jessica Kolhmann

Moreover, solid-state NMR may also unveil information across the “difficult” 0.3–1 nm length-scale, unlike other ...